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Gotardo, E

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(trusted non-journal) U.S

After isolation of the ion m/z 628.3, the recorded MS 3 spectrum showed specific fragment ions indicating the cleavage of the amino acid valine ( m/z 628.3 [M+K] + 528.2, [M+K] + ) or the dipeptide L- O -Val-L-Val ( m/z 628.3 [M+K] + 427.1 [M+K] + ) to release the tetradepsipeptide L- O -Val-L-Val-D- O -Leu-D-Ala which could also be detected in the MS 4 spectrum after isolation of the fragment ion m/z 528.2

At present, it is not known both what is the primum movens responsible for APE1/Ref-1 gene expression upon oxidative stress and the signalling pathways leading to its activation